Table 4: Validation results in milk.
| Compound | Accuracy (%) at 0.5-1-2 MRL/RC (n = 8) | CV (%) at 0.5-1-2 MRL/RC (n = 8) | Linearity r2 | CCα (μg/kg) | CCβ (μg/kg) | LOQ (μg/kg) |
| 4MAA | 89-91-90 | 10-4-6 | 0.98 | 53 | 56 | 25 |
| TLF | 96-97-101 | 96-97-101 | 0.93 | 62 | 74 | 25 |
| DCL | 99-92-96 | 12-10-9 | 0.97 | 0.12 | 0.13 | 0.05 |
| CPF | 103-102-97 | 8-4-5 | 0.99 | 532 | 564 | 250 |
| PBZ | 87-89-95 | 12-6-11 | 0.96 | 2.50 | 3 | 2.5 |
| FLU-OH | 102-104-105 | 9-8-11 | 0.97 | 46 | 51 | 20 |
| MLX | 97-101-98 | 6-5-6 | 0.99 | 16 | 18 | 7.5 |
| IBU | 102-108 | 8-9-13 | 0.96 | 5.00 | 7 | 5 |
| CAP | 104-99-101 | 10-3-6 | 0.99 | 0.15 | 0.17 | 0.15 |