Table 5: Results of robustness study of FVS.
Parameter variation |
Recovery % ± SDa |
|
Initial rate |
Fixed time |
|
No Change |
100.75 ± 0.38 |
100.33 ± 0.32 |
MBTH (0.01 M) volume (± 0.1 mL) |
||
0.90 mL |
98.90 ± 0.23 |
98.96 ± 0.24 |
1.10 mL |
99.05 ± 0.16 |
99.32 ± 0.21 |
Ce(SO4)2 (1% w/v) volume (± 0.1 mL) |
||
0.90 mL |
98.46 ± 0.26 |
98.60 ± 0.14 |
1.10 mL |
98.27 ± 0.14 |
98.30 ± 0.12 |
Measurement time (± 5.0 min) |
||
10 min |
99.49 ± 0.13 |
99.58 ± 0.09 |
20 min |
99.89 ± 0.15 |
100.03 ± 0.11 |
aAverage of five determinations. |